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1,10-DECAMETHYLENE DIBROMIDE

1,10-Dibromodecane

CAS: 4101-68-2

Molecular Formula: C10H20Br2

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1,10-DECAMETHYLENE DIBROMIDE - Names and Identifiers

Name 1,10-Dibromodecane
Synonyms Dibromodecane
1,10-DIBROMODECANE
1,10-Dibromodecane
TIMTEC-BB SBB008900
1,10-DECANE DIBROMIDE
DECAMETHYLENE BROMIDE
DECAMETHYLENE DIBROMIDE
Decamethylene dibromide
1,10-DECAMETHYLENE BROMIDE
1,10-DECAMETHYLENE DIBROMIDE
CAS 4101-68-2
EINECS 223-871-0
InChI InChI=1/C10H20Br2/c11-9-7-5-3-1-2-4-6-8-10-12/h1-10H2
InChIKey GTQHJCOHNAFHRE-UHFFFAOYSA-N

1,10-DECAMETHYLENE DIBROMIDE - Physico-chemical Properties

Molecular FormulaC10H20Br2
Molar Mass300.07
Density1.335 g/mL at 25 °C (lit.)
Melting Point25-27 °C (lit.)
Boling Point160 °C/15 mmHg (lit.)
Flash Point26°C
Water Solubilityinsoluble
Vapor Presure0.00233mmHg at 25°C
AppearanceWhite crystal
Specific Gravity1.335
ColorBeige to brown
BRN506156
Storage ConditionSealed in dry,Room Temperature
SensitiveEasily absorbing moisture
Refractive Indexn20/D 1.4912(lit.)
MDLMFCD00000222
Physical and Chemical PropertiesWhite flaky crystals. Melting point 27 ℃(25.5-26 ℃), boiling point 161-162.4 ℃(1.2kPa),110 ℃(4 × 10-2kPa), relative density 1.335(30/4 ℃), refractive index 1.4905(30 degrees C). Soluble in ethanol, slightly soluble in cold ethanol, insoluble in water. Deliquescence.
UseUsed as an intermediate in organic synthesis.

1,10-DECAMETHYLENE DIBROMIDE - Risk and Safety

Risk CodesR20/21/22 - Harmful by inhalation, in contact with skin and if swallowed.
R36/37/38 - Irritating to eyes, respiratory system and skin.
Safety DescriptionS22 - Do not breathe dust.
S24/25 - Avoid contact with skin and eyes.
S36 - Wear suitable protective clothing.
S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice.
WGK Germany3
TSCAYes
HS Code29049090

1,10-DECAMETHYLENE DIBROMIDE - Introduction

Soluble in ethanol, slightly soluble in cold ethanol, insoluble in water. Easy deliquescence.
Last Update:2022-10-16 17:25:08

1,10-DECAMETHYLENE DIBROMIDE - Reference Information

NIST chemical information Information provided by: webbook.nist.gov (external link)
EPA chemical information Information provided by: ofmpub.epa.gov (external link)
Use Used as an intermediate in organic synthesis.
Production method It is obtained by the reaction of decanediol and hydrogen bromide. Heat decanediol to 95-100°C, and pass in dry hydrogen bromide gas under stirring. When the hydrogen bromide in the mixture is saturated, the temperature is raised to 135 ℃, and hydrogen bromide is slowly introduced. Cooling, dividing the water layer to obtain the coarse product. Wash with water, then wash with 10% sodium carbonate solution, remove all the acid and then carry out reduced pressure distillation, collect 139-142 ℃(0.266kPa) fraction to obtain the finished product.
Last Update:2024-04-10 22:29:15
1,10-DECAMETHYLENE DIBROMIDE
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View History
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